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Beilstein J. Org. Chem. 2017, 13, 1816–1822, doi:10.3762/bjoc.13.176
Graphical Abstract
Scheme 1: Reaction process.
Figure 1: ORTEP drawing of Z-4ai.
Scheme 2: Reaction mechanism.
Scheme 3: Isomerization of the stereochemistry of 4ai.
Scheme 4: Reaction of cycloalkane-1,2-diones with phenyl vinyl ketone (6a).
Scheme 5: Preparation and reactivity of the bisacylated Breslow intermediate 10.
Figure 2: ORTEP drawing of 10.
Scheme 6: Preparation of the iminium salt 12 and its reactivity.
Scheme 7: Resting state of the monoacylated Breslow intermediate C.